Study on the strength deterioration characteristics and microscopic mechanisms of moraine soil under freeze-thaw cycles
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Abstract: To investigate the strength degradation characteristics and microscopic damage mechanisms of moraine soil under hydro-thermo-mechanical coupling conditions, a series of X-ray Diffraction (XRD), standard triaxial testing, Scanning Electron Microscopy (SEM), and Nuclear Magnetic Resonance (NMR) experiments were conducted. The mechanical property degradation laws and evolution characteristics of the microscopic pore structure of moraine soil under Freeze-Thaw (F-T) conditions were revealed. After F-T cycles, the stress-strain curves of moraine soil showed a strain-softening trend. In the early stage of F-T cycles (0–5 cycles), the shear strength and elastic modulus exhibited damage rate of approximately 10.33% ± 0.8% and 16.60% ± 1.2%, respectively. In the later stage (10–20 cycles), the strength parameters fluctuated slightly and tended to stabilize. The number of F-T cycles was negatively exponentially correlated with cohesion, while showing only slight fluctuation in the internal friction angle, thereby extending the Mohr-Coulomb strength criterion for moraine soil under F-T cycles. The NMR experiments quantitatively characterized the evolution of the internal pore structure of moraine soil under F-T cycles. As the number of F-T cycles increased, fine and micro pores gradually expanded and merged due to the frost-heaving effect during the water-ice phase transition, forming larger pores. The proportion of large and medium pores increased to 59.55% ± 2.1% (N=20), while that of fine and micro pores decreased to 40.45% ± 2.1% (N=20). The evolution of pore structure characteristics was essentially completed in the later stage of F-T cycles (10–20 cycles). This study provides a theoretical foundation and technical support for major engineering construction and disaster prevention in the Qinghai-Xizang Plateau.
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Figure 4. The stress-strain curve of moraine under F-T cycle (a. $ {\sigma _{\text{3}}} = $100 kpa, $ w = $10.7%, b. $ {\sigma _{\text{3}}} = $100 kpa, $ w = $14.1%, c. $ {\sigma _{\text{3}}} = $100 kpa, $ w = $18%, d. $ {\sigma _{\text{3}}} = $150 kpa, $ w = $10.7%, e. $ {\sigma _{\text{3}}} = $150 kpa, $ w = $14.1%, f. $ {\sigma _{\text{3}}} = $150 kpa, $ w = $18%, g. $ {\sigma _{\text{3}}} = $200 kpa, $ w = $10.7%, h. $ {\sigma _{\text{3}}} = $200 kpa, $ w = $14.1%, i. $ {\sigma _{\text{3}}} = $200 kpa, $ w = $18%)
Figure 11. The multi-parameter coupling model for mechanical characteristics of moraine soil (a. the relationship surface among shear strength, number of F-T cycles and initial moisture content, b. the relationship surface among elastic modulus, the number of F-T cycles and initial moisture content, c. the relationship surface among shear strength, number of F-T cycles and confining pressure, d. the relationship surface among elastic modulus, number of F-T cycles and confining pressure)
Figure 12. The microstructure of moraine soil under different F-T cycles (a. N=0 and the magnification of 100×, b. N=0 and the magnification of 200×, c. N=10 and the magnification of 100×, d. N=10 and the magnification of 200×, e. N=20 and the magnification of 100×, f. N=20 and the magnification of 200×)
Table 1. The basic physical parameters of moraine soil
Dry density
$ {\rho _d} $/(g/cm3)Unit weight
$ \gamma $/(kN/m3)Optimum moisture
content $ {w_o} $/(%)Maximum dry
density $ {\rho _{d\max }} $/(g/cm3)Nonuniform
coefficient $ {C_u} $Curvature
coefficient $ {C_c} $1.7 26.1 14.1% 2.30 2.20 0.94 Table 2. The experimental scheme
Experiment name Moisture Content
w/%Confining Pressure
σ3/kPaNumber of F-T Cycle N Number of Samples Consolidated undrained triaxial test (CU) 10.7
14.1
18
100,150,200
0,2,5,10,15,20
162NMR Moisture Content w/% Number of F-T Cycle N Number of Samples 10.7 0,2,5,10,15,20 18 SEM Moisture Content w/% Magnification power Number of F-T Cycle N Number of Samples 10.7 100×、200× 0,2,5,10,15,20 6 Table 3. Quantitative analysis of microstructure from SEM images
Number of F-T
Cycles/NPorosity/% Average Pore
Diameter/μm0 15.2 ± 0.8 8.5 ± 0.5 10 22.7 ± 1.2 14.1 ± 0.7 20 28.9 ± 1.5 18.6 ± 0.9 Table 4. The pore classification table
The pore
classificationLarge pores Medium pores Small pores Micropores Size/μm >100 100–30 30–3 <3 Table 5. Evolution of micro-pore structure parameters of moraine soil
N Large-medium pore/% $ {D_f} $ $ {d_{avg}} $ 0 0.00 2.68±0.05 8.2±0.4 20 59.55±2.1 2.31±0.06 21.5±1.1 -
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